Explore the pioneering field of Nanostatistics, where data science, nanotechnology, and machine learning converge, with Fernando Gomes de Souza Junior as your guide. In this book, Dr Souza Junior, a respected authority in the field, provides an in-depth introduction to this transformative discipline, revolutionizing our understanding of nanomaterials and their behaviors. This book is a testament to the power of Design of Experiments (DoE), advanced statistical models, and artificial intelligence in addressing real-world challenges in sustainability, healthcare, and technology. The case studies, rooted in authentic nanotechnology scenarios, feature datasets generated through Monte Carlo simulations, offering a controlled yet realistic framework for tackling complex nanoscale problems. Organized into fourteen comprehensive sections, the book underscores the interdisciplinary nature of data-driven nanotechnology. It highlights the ethical responsibilities of data innovation and the collaborative spirit essential to navigating this transformative field. Whether you are an academic, practitioner, or student, this book equips you with the tools to explore the statistical frontiers of nanotechnology and contribute to a community shaping the future at the nanoscale.